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Identity HelpUnknown crystal from Afghanistan
22nd Feb 2019 18:01 UTCNick Gilly
I bought the following crystal as an unknown from one of the Peshawar sellers on eBay. It's apparently from Badakhshan Province, Afghanistan, maybe from the Deo-Darrah pegmatite? The crystal is 4.8 cm long, by 2.7 cm 1.7 cm. When I first saw the pics I wondered if it was topaz, but now I have the specimen here, it's clear it isn't. It has a 6-sided cross-section, is vertically striated and has cleavage planes showing in 2 directions I think. It feels quite dense, comparable to topaz, so the SG I would estimate to be around 3.5. It weighs 33 grams to the nearest whole number. The crystal shows some weak peach-coloured fluorescence using my cheap 395 nm UV torch. It scratches glass but needs a bit of pressure to make a clear scratch, so I'd estimate hardness to be around 6. It looks like it may crystallise in the monoclinic system. Here's some pics from the auction below:
[img]https://i.ebayimg.com/images/g/uYwAAOSwXyBcU0sY/s-l1600.jpg[/img]
[img]https://i.ebayimg.com/images/g/-08AAOSw3-9cU0re/s-l1600.jpg[/img]
[img]https://i.ebayimg.com/images/g/yBwAAOSwf0hcU0sm/s-l1600.jpg[/img]
[img]https://i.ebayimg.com/images/g/bVoAAOSwRKVcU0uK/s-l1600.jpg[/img]
[img]https://i.ebayimg.com/images/g/WxoAAOSwdgxcU0ur/s-l1600.jpg[/img]
[img]https://i.ebayimg.com/images/g/jmwAAOSwptZcU0u5/s-l1600.jpg[/img]
It's maybe not that clear from the images but the crystal has a pale yellowish-greenish tinge. It's a handsome specimen.
So, any suggestions most welcome.
Thanks
22nd Feb 2019 18:36 UTCFrank K. Mazdab 🌟 Manager
22nd Feb 2019 19:23 UTCNick Gilly
From a couple of angles there is also a clear chatoyancy/schiller type effect, as if there are parallel fibres or very thin tubes reflecting the light internally. I don't know if this helps.
22nd Feb 2019 20:01 UTCFrank K. Mazdab 🌟 Manager
22nd Feb 2019 20:27 UTCJosé Zendrera 🌟 Manager
Six sided section could be an octagonal section in which two faces are missing. Vertical striation, luster, color, interior fractures and yellow fluorescence under long wave (with a filtered 365 nm lamp) are in accord with marialite.
Nick, can you check fluorescence under short wave? it should be red in marialite from Badakhshan.
Also can check the angles between prism faces. If it's hexagonal you will find 120º. Marialite can have 135º and 90º
22nd Feb 2019 20:38 UTCNick Gilly
Using a protractor the angles look close to 90º and 130º. I think it's slightly less than 90º and slightly more than 130º, so that may mean it's not tetragonal.
22nd Feb 2019 20:45 UTCErik Vercammen Expert
22nd Feb 2019 21:49 UTCNick Gilly
It probably is a pyroxene of some sort.
22nd Feb 2019 22:37 UTCNick Gilly
https://www.ebay.co.uk/itm/228-CT-Florescent-Full-Terminated-Natural-Color-Unusual-Unknown-Huge-Crystal-AFG-/273599807983?hash=item3fb3d1c1ef%3Ag%3AE4QAAOSwSlpcCugd&nma=true&si=ixjQQNnReTNMiRRT05C3KlM5GqA%253D&orig_cvip=true&nordt=true&rt=nc&_trksid=p2047675.l2557
Some more useful info that will hopefully help with an ID.
22nd Feb 2019 22:51 UTCScott Rider
This one is tricky, and could be a number of different minerals. But I was also thinking spodomene as well...
However, my very first gut feeling was it is richterite. Mostly because I was holding one the other day that has similar clarity, color and striations, but not the termination. I scoured a TON of images of that and have found none that have that termination. I can't seem to find a text book schematic of the mineral and am not too familiar with the mineral.
Whatever it is, sure is a good looking crystal with a decent termination... If it is a pyroxene, then that is a REALLY good sample.
https://www.minerals.net/Image/15/202/Zoisite.aspx
22nd Feb 2019 22:56 UTCNick Gilly
If it is richterite, then it's a damn good one! I'd be amazed if it was though. Probably something more mundane.
23rd Feb 2019 03:13 UTCIan Nicastro
23rd Feb 2019 04:26 UTCPaul Brandes 🌟 Manager
23rd Feb 2019 05:30 UTCFrank K. Mazdab 🌟 Manager
This "dilemma" could also easily be solved with a simple precise density measurement. Even to just one decimal place, marialite has a density of 2.5 to 2.6 g/cm3... all of the other choices that have been mentioned (richterite, spodumene, zoisite/clinozoisite) have densities between 3.1 and 3.4 g/cm3. A better cleavage determination would also be definitive to differentiate between scapolite, pyroxene, amphibole and the epidote group, but of course it's neither practical nor desirable to produce fresh cleavage surfaces on this particular nice crystal.
23rd Feb 2019 07:13 UTCDoug Daniels
23rd Feb 2019 07:31 UTCFrank K. Mazdab 🌟 Manager
23rd Feb 2019 07:51 UTCNick Gilly
I don't have an accurate balance to calculate SGs (the one in our kitchen only displays to the nearest whole gram) but for those suggesting a scapolite I can eliminate that possibility. The listed SG range for marialite-meonite is 2.5-2.78, so if it was a scapolite it would have the same sort of light feel as a quartz crystal. This specimen is definitely denser than that, and feels heavy, like a topaz. So I'm pretty sure it's not a scapolite.
Here's a really quick view of the termination from above, if it helps:
23rd Feb 2019 08:06 UTCFrank K. Mazdab 🌟 Manager
This 200g balance (±0.01g) costs under $6... no one's bank will be broken:
https://www.ebay.com/itm/Portable-200g-x-0-01g-Mini-Digital-Scale-Jewelry-Pocket-Balance-Weight-Gram-LCD/302976550494?_trkparms=aid%3D555018%26algo%3DPL.SIM%26ao%3D1%26asc%3D20131003132420%26meid%3Ddb7c8f7016d34680a6e22f48170b5004%26pid%3D100005%26rk%3D10%26rkt%3D12%26mehot%3Dag%26sd%3D332701401811%26itm%3D302976550494&_trksid=p2047675.c100005.m1851
23rd Feb 2019 08:57 UTCNick Gilly
I'm still hoping to get further tests done on this specimen though as I would like a confirmed ID.
Edit: Frank thanks for the link to that balance. I didn't realise they could be bought that cheap!
23rd Feb 2019 09:46 UTCFrank K. Mazdab 🌟 Manager
23rd Feb 2019 11:14 UTCNick Gilly
I'm going with diopside for now.
24th Feb 2019 21:36 UTCMichael Christensen
25th Feb 2019 07:28 UTCIan Nicastro
25th Feb 2019 15:17 UTCNick Gilly
There's a mineral show this coming weekend which always has some dealers from Afghanistan or Pakistan. I'll be taking this crystal with me, as well as the suspected bastnäsite specimen. I know they've also had people there with testing equipment in the past, so someone may be able to held ID them.
25th Feb 2019 17:41 UTCFrank K. Mazdab 🌟 Manager
25th Feb 2019 19:40 UTCNick Gilly
26th Feb 2019 01:21 UTCFrank K. Mazdab 🌟 Manager
As for hardness, that's a test that's frequently not done well (works best with a set of hardness test points, which few people use)... in any case, you noted it scratched glass but didn't mention whether it also scratched quartz or if quartz scratches it (on the discreet base), even if some good amount of pressure is needed. Your fifth photo seems to show the classic basal cleavage, and your density estimate (admittedly also a test not often done well, especially when done by just 'heft" and not quantitatively) is self-described as consistent with topaz.
It will be interesting to hear what the dealers at your upcoming local mineral show think about this crystal, as well as subsequently when you're able to obtain some near-term quantitative density data (after you buy a $6 scale) and any possible future chemical or optical data you're able to get.
26th Feb 2019 08:59 UTCNick Gilly
It doesn't scratch quartz, so my hardness estimate of 6 stands. It also appears to show cleavage planes in 2 directions. So for me, that rules out topaz.
26th Feb 2019 20:02 UTCIan Nicastro
26th Feb 2019 20:04 UTCNick Gilly
26th Feb 2019 20:47 UTCFrank K. Mazdab 🌟 Manager
And as an aside, several posters have noted, "is consistent with the locality". What locality? Nick said "apparently from Badakhshan province". Badakhshan not a deposit... it's a region of 44,000 km2 (that's about the size of Switzerland, and probably as geologically diverse). Half the minerals in mindat are likely consistent with that locality. As for "maybe from Deo-Darrah pegmatite"... did the seller say "maybe from" or is Nick saying "maybe from"? In either case, "maybe from" only muddies the waters and should not have been included as a clue. Because I bet if the clue were instead, "maybe from Tanzania", there would have been an entirely different set of guesses. Either the specimen "is from ___________" (then a good clue to it's identity because then its geology can be incorporated), or one has an unknown mineral from an unknown locality, and the more fake clues that are added don't help in solving either mystery.
Take it to the nearest university and have a professional examine it live, or better yet, break a tiny chip off the bottom where it can be discreetly done and have it SEMed or X-rayed... then let's put this thread to rest.
28th Feb 2019 07:49 UTCIan Nicastro
28th Feb 2019 09:36 UTCJohan Kjellman Expert
the crystal looks similar to pyroxene (aegirine) crystals depicted in Goldschmidt, vol 7, for example plate 44, fig 18
cheers
28th Feb 2019 10:09 UTCFrank K. Mazdab 🌟 Manager
I think you mis-read what I wrote about the locality. The only thing known (or believed) about the locality is, to quote what Nick originally wrote, "...apparently from Badakhshan Province, Afghanistan, maybe from the Deo-Darrah pegmatite?" It's not clear whether that assessment is Nick's or the dealer's, but because of the qualifiers of both "apparently" and "maybe", those purported localities unfortunately don't help in identifying the mineral... rather, because the true locality isn't actually known, those purported localities only serve to prejudice us into making assumptions about what the mineral could be (because we include or eliminate possibilities based on what we understand of the geology of these places) but that may or may not be true. All we know about the locality, with reasonable but not absolute certainty, is that since the dealer is from Pakistan, the sample is probably from somewhere within a few hundred miles of his home base (which cover 2-3 countries). Unless the dealer offered more concrete information on his listing (I don't know... I didn't see the listing), that really is all we know; so, the dealer didn't acquire it in Africa or South America (probably... lol).
In any case, your suggestions of tremolite and/or herderite are both consistent with the apparent crystallography (indeed, as herderite can appear pseudo-orthorhombic, it's probably even one of the better guesses), and both would seem consistent with some of the other properties as well. So those two additional suggestions can be piled on to the now fairly extensive list of potential identities that include everything but the kitchen sink (but not scapolite [lol], or anything else isometric, tetragonal, hexagonal or trigonal; or anything metallic; or anything one can scratch with their fingernail). Ultimately, when it comes to identifying minerals from a photo, even the most professional of us (including me) are relegated to being just handicapped arm-chair mineralogists. We might offer some good guesses... one or several of us might even end up correct. But ultimately there's no substitute for a professional examining the crystal live in his or her own hands. We can all guess in perpetuity, but in the end we're going to have to wait for Nick's report back from someone at a local museum or university.
28th Feb 2019 10:20 UTCFrank K. Mazdab 🌟 Manager
If the horizontal plane is a cleavage direction (and from the fifth photo it seems that way to me too), then it can't be a pyroxene because the two cleavages in pyroxene are {110} and intersect in the a-b plane, and so would be parallel rather than perpendicular to the long c direction of the crystal (this orientation would be true of amphibole too). However, if the horizontal plane actually isn't a cleavage, then pyroxenes or amphiboles are back on the table.
28th Feb 2019 12:21 UTCPeter Slootweg 🌟
28th Feb 2019 13:35 UTCNick Gilly
The location was just listed as Badakhshan Province, nothing more specific than that. A lot of the specimens listed from there seem to be from the Koksha Valley, and this specimen looked different to most I've seen from there, so the Deo Darrah pegmatite was a guess. I've seen quite a bit of diopside listed from the Koksha Valley (some of them as unknowns too) and these have been bright green, sometimes with lazulite spotting the crystal, making for a nice colour contrast. This specimen is obviously very different in appearance.
The cleavages seem to be in two directions, the horizontal ones slightly offset in both directions from the base, and the vertical one does seem to be directly parallel to the c axis.
The UV response seems to be peach in LW UV, and blue in SW UV (judging from the pics in the other auction). I don't know of any spodumene that fluoresces blue in SW UV, but I could be wrong.
It does look a bit like some specimens of hydroxylherderite I've seen, but I do have a crystal of this material from Brazil, and that doesn't scratch glass. This specimen does.
If it is spodumene it's got a very odd termination.
I'll be taking it to the Kempton Park Rock & Gem Show at the weekend, so maybe we'll get a better idea from some of the dealers there. If not, then I may see if I can get Southampton University to do some Raman spectroscopy on it.
28th Feb 2019 17:37 UTCFrank K. Mazdab 🌟 Manager
since the dealer you bought it from didn't know what it was, it's possible the dealers at the mineral show also won't know (or might also disagree with each other). While it's still probably a worthwhile endeavor to give the dealers at the mineral show a try, if you indeed do know someone at Southampton that can do more sophisticated testing for you, I'd definitely recommend that. The latter option might be especially useful if the mineral turns out to be either very unusual, or it's a member of a series/family (like herderite/hydoxylherderite) where the individual members couldn't be easily distinguished by physical means alone.
28th Feb 2019 17:50 UTCNick Gilly
I will phone Southampton University tomorrow and see if I can get someone there to test it.
1st Mar 2019 17:01 UTCNick Gilly
1st Mar 2019 19:39 UTCFrank K. Mazdab 🌟 Manager
Although it's possible they may send you home with an actual spectrum that you can upload and post here, it's more likely that their instrument connects to a database of Raman spectra (perhaps even the RRUFF database) that compares the spectrum to what's in their database, much like how powder XRD matching is done, and looks for matches.
So it will output a list of potential mineral (and perhaps chemical compound) matches, in order of decreasing probability. You'll want to post the list of the top several matches. As Raman spectra are directional, you (or the instrument technician) might also want to measure the crystals in two or all three principal orientations, if possible, and include those results here too. Then we as the arm-chair mineralogists can consider the minerals on your list(s) in the context of the other properties already posted here (crystallography, hardness, density, color, "locality") to ascertain which of the list entries is most plausible (and while the best answer typically is one of the minerals at the top or close to the top of the list, that's not always guaranteed).
Although posting the actual raw spectrum here might be interesting, few if any of us here have our own Raman databases handy and so we probably wouldn't be able to offer much ID help from the raw data itself. But for those well-versed in Raman spectroscopy, looking at the finer features of the spectrum could offer an entertaining diversion.
1st Mar 2019 22:31 UTCNick Gilly
It looks like it may have to be the week after next now, but fingers crossed. Before then, I'll see what transpires at tomorrow's Rock & Gem Show.
1st Mar 2019 22:35 UTCFrank K. Mazdab 🌟 Manager
2nd Mar 2019 16:39 UTCNick Gilly
I think spodumene is looking likely though. I'll find out for sure when I have it tested at Southampton University.
As an aside, I actually spent very little money at the show but did see one dealer with a parcel of gem rough pink spinel from Tajikistan. I picked out two pieces showing some crystal faces, at the really cheap price of £1/gram, and then a couple more later, by which time the dealer had raised the price to £3/gram lol. Still, 4 small gem partial crystals at a total of £7 is a steal!
20th Mar 2019 18:13 UTCNick Gilly
...diopside!
20th Mar 2019 18:36 UTCScott Rider
20th Mar 2019 18:56 UTCFrank K. Mazdab 🌟 Manager
But a couple of other noteworthy outcomes then are (1) that those horizontal surfaces in several photos that look like a basal cleavage are simply fractures; the well-known near 90° {110} cleavage in pyroxene would be parallel to the length of your crystal. And (2) your crystal isn't from a pegmatite... at least not from any granite pegmatite that would abundant in the region.
20th Mar 2019 18:57 UTCNick Gilly
It's certainly an odd termination for a diopside.
20th Mar 2019 19:49 UTCFrank K. Mazdab 🌟 Manager
20th Mar 2019 20:57 UTCIan Nicastro
20th Mar 2019 21:30 UTCNick Gilly
I think the matrix for the dravite may be feldspar with some calcite as well as the mica. This is based on the fact that quite a few bits scratch glass but there is also a softer mineral intermixed that doesn't. For example there are some crystals adjacent to the dravite that look like they show calcite cleavage faces.
21st Mar 2019 01:25 UTCPaul Brandes 🌟 Manager
Thanks for keeping us in the loop throughout, Nick!
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Copyright © mindat.org and the Hudson Institute of Mineralogy 1993-2024, except where stated. Most political location boundaries are © OpenStreetMap contributors. Mindat.org relies on the contributions of thousands of members and supporters. Founded in 2000 by Jolyon Ralph.
Privacy Policy - Terms & Conditions - Contact Us / DMCA issues - Report a bug/vulnerability Current server date and time: May 14, 2024 01:33:05
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