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Bell, A. M. T., Henderson, C. M. B. (2012) High-temperature synchrotron X-ray powder diffraction study of Cs2XSi5O12(X = Cd, Cu, Zn) leucites. Mineralogical Magazine, 76 (5) 1257-1280 doi:10.1180/minmag.2012.076.5.12

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Reference TypeJournal (article/letter/editorial)
TitleHigh-temperature synchrotron X-ray powder diffraction study of Cs2XSi5O12(X = Cd, Cu, Zn) leucites
JournalMineralogical Magazine
AuthorsBell, A. M. T.Author
Henderson, C. M. B.Author
Year2012 (October)Volume76
Issue5
PublisherMineralogical Society
DOIdoi:10.1180/minmag.2012.076.5.12Search in ResearchGate
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Mindat Ref. ID244283Long-form Identifiermindat:1:5:244283:3
GUID0
Full ReferenceBell, A. M. T., Henderson, C. M. B. (2012) High-temperature synchrotron X-ray powder diffraction study of Cs2XSi5O12(X = Cd, Cu, Zn) leucites. Mineralogical Magazine, 76 (5) 1257-1280 doi:10.1180/minmag.2012.076.5.12
Plain TextBell, A. M. T., Henderson, C. M. B. (2012) High-temperature synchrotron X-ray powder diffraction study of Cs2XSi5O12(X = Cd, Cu, Zn) leucites. Mineralogical Magazine, 76 (5) 1257-1280 doi:10.1180/minmag.2012.076.5.12
Abstract/NotesAbstractSynchrotron X-ray powder diffraction data have been collected on three synthetic leucite analogues with the general formula Cs2XSi5O12(X = Cd, Cu, Zn) between 295 and 1173 K. All three samples have the orthorhombic Pbca leucite structure at room temperature with ordered framework T-site cations. The sample with X = Cd retains the Pbca structure over the whole of the investigated temperature range. The sample with X = Cu also retains the Pbca structure, but there is a transition to a less distorted structure with a larger unit-cell volume at ∼333 K. The sample with X = Zn shows evidence for a transition to a previously unknown Pa cubic structure, with some T-site cation disorder, at 566 K, on heating. This transition is reversible on cooling to 633 K.

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Bell, A. M. T., Henderson, C. M. B. (1994) Rietveld refinement of the structures of dry-synthesized MFeIIISi2O6 leucites (M = K, Rb, Cs) by synchrotron X-ray powder diffraction. Acta Crystallographica Section C Crystal Structure Communications, 50 (10) 1531-1536 doi:10.1107/s0108270194004014
Ardit, M., Cruciani, G., Dondi, M., Garbarino, G. L., Nestola, F. (2014) Phase transitions during compression of thaumasite, Ca3Si(OH)6(CO3)(SO4)·12H2O: A high-pressure synchrotron powder X-ray diffraction study. Mineralogical Magazine, 78 (5) 1193-1208 doi:10.1180/minmag.2014.078.5.07
Leardini, L., Martucci, A., Braschi, I., Blasioli, S., Quartieri, S. (2014) Regeneration of high-silica zeolites after sulfamethoxazole antibiotic adsorption: a combined in situ high-temperature synchrotron X-ray powder diffraction and thermal degradation study. Mineralogical Magazine, 78 (5) 1141-1159 doi:10.1180/minmag.2014.078.5.04
Reece, J. J., Redfern, S. A. T., Welch, M. D., Henderson, C. M. B. (2000) Mn-Mg disordering in cummingtonite: a high-temperature neutron powder diffraction study. Mineralogical Magazine, 64 (2) 255-266 doi:10.1180/002646100549166
Grangeon, S., Lanson, B., Lanson, M., Manceau, A. (2008) Crystal structure of Ni-sorbed synthetic vernadite: a powder X-ray diffraction study. Mineralogical Magazine, 72 (6) 1279-1291 doi:10.1180/minmag.2008.072.6.1279
Beagley, B., Henderson, C. M. B., Taylor, D. (1982) The crystal structures of aluminosilicate-sodalites: X-ray diffraction studies and computer modelling. Mineralogical Magazine, 46 (341) 459-464 doi:10.1180/minmag.1982.046.341.09
Henderson, C. M. B., Bell, A. M. T., Charnock, J. M., Knight, K. S., Wendlandt, R. F., Plant, D. A., Harrison, W. J. (2009) Synchrotron X-ray absorption spectroscopy and X-ray powder diffraction studies of the structure of johnbaumite [Ca10(AsO4)6(OH,F)2] and synthetic Pb-, Sr- and Ba-arsenate apatites and some comments on the crystal chemistry of the apatite structure type in general. Mineralogical Magazine, 73 (3) 433-455 doi:10.1180/minmag.2009.073.3.433
Sameshima, T., Henderson, G. S., Black, P. M., Rodgers, K. A. (1985) X-ray diffraction studies of vivianite, metavivianite, and barićite. Mineralogical Magazine, 49 (350) 81-85 doi:10.1180/minmag.1985.049.350.11
Line, C. M. B., Dove, M. T., Knight, K. S., Winkler, B. (1996) The low-temperature behaviour of analcime. 1: high-resolution neutron powder diffraction. Mineralogical Magazine, 60 (400) 499-507 doi:10.1180/minmag.1996.060.400.11
Bell, A. M. T., Henderson, C. M. B. (1996) Rietveld refinement of dry-synthesized Rb2ZnSi5O12 leucite by synchrotron X-ray powder diffraction. Erratum. Acta Crystallographica Section C Crystal Structure Communications, 52 (2) 490 doi:10.1107/s0108270196099775
Bell, A. M. T., Henderson, C. M. B. (1994) Rietveld refinement of dry-synthesized Rb2ZnSi5O12 leucite by synchrotron X-ray powder diffraction. Acta Crystallographica Section C Crystal Structure Communications, 50 (7) 984-986 doi:10.1107/s0108270194002039
 
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